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KMID : 0381919990290030281
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Korean Journal of Microscopy
1999 Volume.29 No. 3 p.281 ~ p.289
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Thixoforming Characteristics of Metal Matrix Composites (Phase identification of $SiC_p/AZ91HP$ Mg composite)
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Lee Jung-Il
Kim Young-Jig
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Abstract
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The stirred and thixoformed $SiC_p/AZ91HP$ Mg composites are studied on the basis of microstructural analysis using transmission electron microscopy (TEM). The products of interfacial reaction are identified as $Mg_2Si$, MgO and $Mg_{17}Al_{12}$ phases and the crystallized phases are found to be orthorhmbic $Al_6Mn$ and decagonal T phases. It is shown that $Mg_2Si$ and $Mg_{17}Al_{12}$ phases are found at the surface of $SiC_p$ and $Al_6Mn$ is found near interface and crystallized on the matrix. Phase identification is carried out by crystallographic work based on primitive cell volume, zero order Laue zone (ZOLZ) patterns and single convergent beam electron diffraction (CBED) patterns containing higher order Laue zone ring from a nanosized region.
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KEYWORD
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$SiC_p/AZ91HP$ Mg composite, Thixoforming, Convergent beam electron diffraction, Primitive cell volume calculation
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